GAZI UNIVERSITY INFORMATION PACKAGE - 2019 ACADEMIC YEAR

COURSE DESCRIPTION
ANALYTICAL METHOD VALIDATION/AKİ-3030
Course Title: ANALYTICAL METHOD VALIDATION
Credits 2 ECTS 8
Course Semester 1 Type of The Course Compulsory
COURSE INFORMATION
 -- (CATALOG CONTENT)
 -- (TEXTBOOK)
 -- (SUPPLEMENTARY TEXTBOOK)
 -- (PREREQUISITES AND CO-REQUISITES)
 -- LANGUAGE OF INSTRUCTION
  Turkish
 -- COURSE OBJECTIVES
 -- COURSE LEARNING OUTCOMES
Knows analytical method development
Knows the validation parameters of analytical methods
Knows statistical methods for analytical method validation
Have knowledge about statistical methods used in analytical chemistry
 -- MODE OF DELIVERY
  The mode of delivery of this course is Face to face
 --WEEKLY SCHEDULE
1. Week  Regulations and quality control standards
2. Week  Analytical method development Error sources (fixed and random errors), significant figures
3. Week  Analytical method validation and validation parameters
4. Week  Specificity, calibration, linear range, range
5. Week  Interferences, standard addition method, external calibration and use of internal standard
6. Week  Accuracy, precition, repeatability, reproducibility, robustness
7. Week  Detection limit, quantitation limit, recovery, standart reference materials.
8. Week  Statistical methods used to calculate the validation parameters (t-test, f-test)
9. Week  Statistical methods used to calculate the validation parameters (t test, f test)
10. Week  Statistical methods used to calculate the validation parameters (Q test, Grubb testi, Cohran testi) Horwitz Rate)
11. Week  Processing and Evaluation of Statistical Data
12. Week  Processing and Evaluation of Statistical Data
13. Week  Revalidation cycle
14. Week  Validation report and other documentation
15. Week  
16. Week  
 -- TEACHING and LEARNING METHODS
 -- ASSESSMENT CRITERIA
 
Quantity
Total Weighting (%)
 Midterm Exams
1
30
 Assignment
1
15
 Application
0
0
 Projects
1
15
 Practice
0
0
 Quiz
0
0
 Percent of In-term Studies  
60
 Percentage of Final Exam to Total Score  
40
 -- WORKLOAD
 Activity  Total Number of Weeks  Duration (weekly hour)  Total Period Work Load
 Weekly Theoretical Course Hours
14
2
28
 Weekly Tutorial Hours
0
 Reading Tasks
14
4
56
 Searching in Internet and Library
14
4
56
 Material Design and Implementation
0
 Report Preparing
4
6
24
 Preparing a Presentation
2
9
18
 Presentation
2
2
4
 Midterm Exam and Preperation for Midterm Exam
1
6
6
 Final Exam and Preperation for Final Exam
1
8
8
 Other (should be emphasized)
0
 TOTAL WORKLOAD: 
200
 TOTAL WORKLOAD / 25: 
8
 Course Credit (ECTS): 
8
 -- COURSE'S CONTRIBUTION TO PROGRAM
NO
 PROGRAM LEARNING OUTCOMES
1
2
3
4
5
1X
2X
3X
4X
5
6X
7X
8X
9X
10
11X
12X
13X
14X
 -- NAME OF LECTURER(S)
   (Doç. Dr. AYSEL BERKKAN(PEHLİVAN))
 -- WEB SITE(S) OF LECTURER(S)
   ( www.gazi.edu.tr/~aysele)
 -- EMAIL(S) OF LECTURER(S)
   (aysele@gazi.edu.tr;ayberkkan@yahoo.com)