GAZI UNIVERSITY INFORMATION PACKAGE - 2019 ACADEMIC YEAR

COURSE DESCRIPTION

STRUCTURE ELUCIDATION BY SPECTRAL METHODS-I/FKİ-3120

Course Title:	STRUCTURE ELUCIDATION BY SPECTRAL METHODS-I
Credits	2	ECTS	5
Course Semester	1	Type of The Course	Elective

COURSE INFORMATION

-- (CATALOG CONTENT)

-- (TEXTBOOK)

-- (SUPPLEMENTARY TEXTBOOK)

-- (PREREQUISITES AND CO-REQUISITES)

-- LANGUAGE OF INSTRUCTION

Turkish

-- COURSE OBJECTIVES

-- COURSE LEARNING OUTCOMES

Be able to explain the basic fundamental principles of MS, IR, NMR spectrometry.
Be able to combine spectroscopic data obtain from different techniques with respect to determining the structure of a organic compound.
Be able to report spectral data in a scientific report.

-- MODE OF DELIVERY

The mode of delivery of this course is face to face

--WEEKLY SCHEDULE
1. Week	General information about IR, NMR, Mass spectroscopy
2. Week	Analysis of first-order spin systems (examples, answers)
3. Week	Analysis of Mass, IR, 1H-NMR, 13C/DEPT spectrums of 3-butyn-1-ol
4. Week	Analysis of Mass, IR, 1H-NMR, 13C/DEPT, COSY, HMQC spectrums of ethyl sorbat
5. Week	Analysis of Mass, IR, 1H-NMR, 13C/DEPT, COSY, HMQC, HMBC spectrums of thymol
6. Week	Structure elucidation of compounds by IR, 1H-NMR, 13C-NMR, Mass spectrums (Problems 1-10)
7. Week	Discussion of homework questions (Problems 11-20)
8. Week	Spectral Analysis of 3-methyl-3-oxetanemethanol(Mass, IR, 1H-NMR, 13C/DEPT, COSY, HMQC, HMBC spectrums)
9. Week	Spectrums of heterocyclic compounds (Problem 21-30)
10. Week	Spectral analysis of substituted benzene derivatives (Problem 31-40)
11. Week	Problems and answers of straight chain compounds with functional groups (Problem 41-45)
12. Week	Spectral analysis of alicyclic compounds (Problem 46-50)
13. Week	1H-19F, 13C-19F coupling constants of aromatic compounds, questions and answers
14. Week	Reporting spectral data in a scientific report
15. Week
16. Week

-- TEACHING and LEARNING METHODS

-- ASSESSMENT CRITERIA

	Quantity	Total Weighting (%)
Midterm Exams	1	60
Assignment	1	20
Application	0	0
Projects	0	0
Practice	0	0
Quiz	5	20

Percent of In-term Studies		40
Percentage of Final Exam to Total Score		60

-- WORKLOAD

Activity	Total Number of Weeks	Duration (weekly hour)	Total Period Work Load
Weekly Theoretical Course Hours	14	2	28
Weekly Tutorial Hours			0
Reading Tasks	4	3	12
Searching in Internet and Library	4	4	16
Material Design and Implementation			0
Report Preparing	3	6	18
Preparing a Presentation	3	5	15
Presentation	1	2	2
Midterm Exam and Preperation for Midterm Exam	1	7	7
Final Exam and Preperation for Final Exam	2	10	20
Other (should be emphasized)			0
TOTAL WORKLOAD:			118
TOTAL WORKLOAD / 25:			4.72
Course Credit (ECTS):			5

-- COURSE'S CONTRIBUTION TO PROGRAM

NO	PROGRAM LEARNING OUTCOMES	1	2	3	4	5
1				X
2				X
3					X
4					X
5						X
6					X
7					X
8					X
9					X
10				X
11		X
12		X
13						X
14		X
15						X
16						X

-- NAME OF LECTURER(S)

(Assoc. Prof. Burcu ÇALIŞKAN)

-- WEB SITE(S) OF LECTURER(S)

(http://websitem.gazi.edu.tr/site/bcaliskan)

-- EMAIL(S) OF LECTURER(S)

( bcaliskan@gazi.edu.tr)

Gazi University

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GAZI UNIVERSITY INFORMATION PACKAGE - 2019 ACADEMIC YEAR